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AbstractCobalt-encapsulated in nitrogen-doped carbon nanotubes (Co-NCNT) were prepared by hydrothermal method. CoCl2·6H2O and graphitic carbon nitride (g-C3N4) were used as raw material. Samples containing such defective structures were synthesized by hydrothermal methods, while there is an excellent synergistic effect between cobalt nanoparticles and carbon nanotubes on hydrogen evolution reaction (HER). In order to improving the HER performance, different samples were fabricated by changing the molar ratio of raw materials and pyrolysis temperature. The results show that Co-NCNT has the best HER performances at the ratio of CoCl2·6H2O and g-C3N4 (1:7) when the pyrolysis temperature reached 700?°C. The overpotential has reached 285?mV when the current density is 10?mA·cm?2, the Tafel slope of the sample is 103?mV·dec?1. 相似文献
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AbstractTi(C,N) ceramic materail plays an important role in the field of material processing due to their good mechanical properties and thermal stability. In this experiment, Ti(C,N) powders were successfully prepared by solvothermal and high-temperature calcining method, using TiOSO4 and C3H6N6 as raw material, and n-propanol and ethylene glycol as solvents. The microstructure of Ti(C,N) powders were characterized by X-ray diffraction and field emission scanning electron microscope, and their hardness were tested by vickers microhardness tester. The microstructure and mechanical properties of Ti(C,N) powders using two different solvents were investigated comparatively. Ti(C,N) powders prepared using n-propanol with a size of about 20–30?μm can reach the maximum hardness of 660 HV after sintering. Ti(C,N) powders prepared using ethylene glycol with size range of 3?μm to 5?μm come up to the maximum hardness of 889 HV. The different mechanism of solvents in preparation of Ti(C,N) ceramic material was discussed. 相似文献
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科学合理的战备完好性评估对于准确掌握部队实战能力,优化保障体系结构,提高装备作战能力与保障效能具有重要意义。针对现有评估模型注重维修保障因素而忽略供应保障因素、无法处理结构和状态较复杂的装备体系与保障体系问题,提出一种新的综合考虑多种保障因素的作战任务间歇期战备完好率评估模型。分析装备体系与保障体系之间的交互关系和保障过程,从装备保障需求角度出发构建装备体系中单个装备作战单元的战备完好率评估模型,在此基础上进一步构建共享同一保障体系多个装备作战单元的战备完好率评估模型。该模型考虑了装备作战单元装备保障需求相同与不同两种情况,并针对模型求解时装备体系状态难以确定的问题,给出一种基于向量通用函数的装备体系状态确定方法。通过实例分析验证了所提模型定量评估战备完好率的有效性和优越性。 相似文献
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Modeling the flow behavior of a simulated municipal solid waste 总被引:2,自引:0,他引:2
Zili Dai Yu Huang Fuhong Jiang Maosong Huang 《Bulletin of Engineering Geology and the Environment》2016,75(1):275-291
Flow slides in the municipal solid waste (MSW) landfill are common geological disasters that have the potential to cause loss of life, destruction of property, and damage to the natural environment in the surrounding region. In this work, a mixture of peat, kaolin clay and quartz sand was used as a model test material to simulate MSW. A series of physical model tests on MSW simulant flows was carried out to capture the run-out behavior of the waste and analyze its mobility. The testing assembly consisted of a transparent model box, a steel frame and a high-speed camera. Flow failure was induced by lifting up a baffle to cause the MSW simulant to collapse and flow. Images of the flowing mass were taken by the high-speed camera. The series of images clearly displays the propagation of MSW simulant flows. The final profile of the MSW simulant and the shape of the deposition area were observed and measured. The run-out distances, final deposit shapes, flow depth, velocities and angle of reach showed significant variation between test configurations, indicating the strong influence of moisture content on overall mobility. The test results obtained can aid in the prediction of distal reach, flow depth and maximum velocity of solid waste following a landfill slope failure, which are necessary for hazard assessment and mitigation planning, and also to provide physical data for theoretical and numerical model verification. 相似文献